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• W2035964059 abstract "Introduction. Mineral trioxide aggregate (MTA) is one of the most commonly used materials in endodontics. Given its shortcomings, there is an intensive search for new materials. Calcium-silicate phase (CS phase) is a new material synthesized by the method based on a combination of sol-gel process and self-propagation synthesis which can significantly improve setting time through accelerated hydration. The aim of this study was to explain the mechanisms of hardening of CS phase in aqueous medium as similar mechanism is expected in contact with body fluids. Materials and Methods. CS phases Ca3SiO5 (C3S) and 2?-CaSiO4 (?-C2S) were synthesized from CaCl2?5H2O (Merck, Germany). To investigate the process of hydration, CS were mixed with water and kept at 37 ?C for 28 days in closed polyethylene containers. Analysis of the composition of samples before and after immersion in water for 1, 3, 7 and 28 days was performed using X - ray diffractometry and IR. Results. XRD patterns for hydrated samples during 1, 3, 7 and 28 days showed that the amount of hydrated tobermorite phases relative to the amount of CS phase changes with the time of hydration. After 1 day, in addition to the hydrated phases, a significant amount of untransformed ?-C2S and C3S were found while after 28 days hydrated CS phase was completely transformed to tobermorite with a small amount of portlandite. Conclusion. Using combined method of sol-gel and self-propagating waves at high temperature very active nanostructured silicate phases were obtained. Hydration process of CS phases was analyzed using XRD and FTIR, the mechanism of hydration was proposed and it was pointed to the difficulties in determining the exact reaction as well as the problem of determining the exact structure of tobermorite." @default.
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• W2035964059 date "2013-01-01" @default.
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• W2035964059 title "Highly active calcium-silicate phases for application in endodontics" @default.
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• W2035964059 doi "https://doi.org/10.2298/sgs1304210j" @default.
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