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- W2036117495 abstract "The oxidation of methanol has been studied over a wide range of concentrations using the electrochemical quartz crystal microbalance (EQCM) technique. Accumulation of strongly adsorbing species at the electrode surface is accompanied by a decrease in mass, relative to the background electrolyte, and the rate of this increase is an indication of how rapidly the surface becomes covered by adsorbates. At lower methanol concentrations, removal of these adsorbates is accompanied by a stepped increase in the mass response and is followed by a small region of potential where the mass is constant and where methanol is apparently oxidized by a reaction with OH at the electrode surface. There is some adsorption in this region too, which increases with increasing methanol concentration. At 30 mM methanol and above, the step upon adsorbate removal and the subsequent region of constant mass can no longer be distinguished. Mass responses also reveal that increasing amounts of methanol in the electrolyte cause a shifting of the oxidative removal of strongly adsorbed intermediates to more positive potentials, a significant inhibition of the irreversible oxidation of the electrode surface and a more rapid removal of the oxide on the cathodic scan." @default.
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- W2036117495 title "Chemisorption and oxidation of methanol at polycrystalline Pt in acid solutions" @default.
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