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• W2036343090 endingPage "508" @default.
• W2036343090 startingPage "498" @default.
• W2036343090 abstract "Cotton fibers were modified by surface-initiated atom transfer radical polymerization of ethyl acrylate (EA) followed by copolymerization with styrene. Either ethyl 2-bromopropionate as a sacrificial free initiator or Cu(II) as a deactivator was used to optimize the EA grafting yield and to preserve the livingness of the chain ends for the subsequent growth of a poly(styrene) (PSty) block from the poly(ethyl acrylate) (PEA) grafts. The polymer-encapsulated cotton fibers were analyzed by Fourier transform infrared spectroscopy, scanning electron microscopy, differential scanning calorimetry (DSC), thermogravimetric analysis, and solid-state NMR (high-resolution 13C cross-polarization magic angle spinning, 1H spin-lattice relaxation times, and 1H free induction decay analysis NMR). The latter allowed the detection of the dynamic modifications associated with the presence of homo- and block copolymer grafts. In particular, the results of the DSC and NMR investigations suggest a heterogeneous morphology of the g-PEA-b-PSty grafted skin, which could be described as an inner layer of g-PEA sandwiched between the semicrystalline cellulose of the core fiber and the high glass transition temperature PSty of the covalently linked outer layer. Such morphology results in a reduced molecular mobility of the PEA chains." @default.
• W2036343090 created "2016-06-24" @default.
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• W2036343090 date "2006-12-24" @default.
• W2036343090 modified "2023-10-18" @default.
• W2036343090 title "Cotton Fibers Encapsulated with Homo- and Block Copolymers: Synthesis by the Atom Transfer Radical Polymerization Grafting-From Technique and Solid-State NMR Dynamic Investigations" @default.
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• W2036343090 doi "https://doi.org/10.1021/bm060602w" @default.
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• W2036343090 hasPublicationYear "2006" @default.
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