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- W2036536422 abstract "A two-stage process involving a thermo-evaporative technique was employed to coat glass capillary columns with polar phases. Silanox 101 and a small amount of liquid phase were introduced in the first stage; additional phase was introduced in the second stage. The theoretical plate efficiency for 5α-cholestane at 250° for a 32 m × 0.25 mm glass column coated with liquid phase PZ-176 was 1800/m. Column properties remained constant when these columns were used between 180° and 320° for the analysis of biologic samples. No indication of deterioration was observed after months of use. Columns made with phase PZ-176 are useful for the separation of long-chain fatty acid methyl esters, polychlorobiphenyls and α-tocopherol as the trimethylsilyl derivative." @default.
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- W2036536422 date "1975-02-01" @default.
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- W2036536422 title "Thermostable glass open tubular capillary columns with a polar liquid phase for gas chromatography" @default.
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- W2036536422 doi "https://doi.org/10.1016/s0021-9673(00)91855-7" @default.
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