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- W2036636038 abstract "Abstract The cubic arsaalkyne tetramer 2 reacts at room temperature with ethyl triflate to give the As‐ethylated arsonium salt 4 . A similar reaction of 2 with benzyl triflate (generated in situ via PhCH 2 Cl/AgOTf) gives the As‐benzylated salt 5 . Low‐temperature protonation of 2 with FSO 3 H/SO 2 produces a mixture of arsonium ions 6 and 7 resulting from mono‐ and diprotonation. The NMR characteristics of the resulting arsonium ions are discussed and compared with those of the corresponding phosphonium ions derived from the tetraphosphacubane 3 . The FAB mass spectrum of 4 and its decomposition products (FAB‐CAD‐MS/M S ) are also discussed." @default.
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- W2036636038 date "1994-09-01" @default.
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- W2036636038 title "Electrophilic chemistry of the cubic arsaalkyne tetramer (AsCtBu)<sub>4</sub>: Arsonium ions of ethylation (EtOTf), benzylation (PhCH<sub>2</sub>OTf), and mono‐ and diprotonation (FSO<sub>3</sub>H/SO<sub>2</sub>)" @default.
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- W2036636038 doi "https://doi.org/10.1002/hc.520050514" @default.
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