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- W2036690018 abstract "Nickel nanoparticle (NiNP) was synthesized by reduction of less toxic nickel acetate tetrahydrate (Ni(CH3CO2)2·4H2O) precursor, using sodium hypophosphite monohydrate (NaPH2O2·H2O) under microwave irradiation. By varying the molar ratio of [Ni+ 2]/[NaPH2O2]/[NaOH], NiNP of 3.8 to 7.1 nm was obtained. Increasing NaOH concentration resulted in morphological change from isolated spherical particles (7.2 ± 1.5 nm) to agglomerated nano flowers (72 ± 14 nm). Phase analysis and interplanar spacing measurements confirmed the particles as fcc-Ni. Quantitative analysis showed the presence of P and O due to HPO2− radical in reaction product. Addition of small amounts of polyvinylpyrolidone (PVP) or cetyltrimethylammonium bromide (CTAB) resulted in slight increase in particle size." @default.
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- W2036690018 date "2012-06-01" @default.
- W2036690018 modified "2023-10-15" @default.
- W2036690018 title "Microwave assisted greener synthesis of nickel nanoparticles using sodium hypophosphite" @default.
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- W2036690018 doi "https://doi.org/10.1016/j.matlet.2012.02.049" @default.
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