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- W2036694945 abstract "Die Umsetzung von Organogermaniumtrihalogeniden mit KCo(CO)4 liefert sowohl die Dreikerncluster RGeCo3(CO)9 (1, R Me, Ph, tBu) als auch die neuen Vierkerncluster (RGe)2Co4(CO)11 (3, R Ph, tBu). Die durch Insertion von Gel2 in Metall-Metall-Bindungen entstehenden Zweikernkomplexe LnM GeI2 MLn (4–6, MLn FeCp(CO)2, Co(CO)4, NiCpCO) setzen sich mit KCo(CO)4 zu den Clustern LnM GeCO3(CO)9 (7–9) um. Metallaustauschreaktionen liefern die Heterovierkerncluster (tBuGe)2Co3(CO)8M′Ln (10, 11, M′Ln MoCp(CO)2, NiCp). Von Cp(CO)2Fe GeCo3(CO)9 (7) und (tBuGe)2Co3(CO)8NiCp (11) wurden Kristallstrukturanalysen durchgeführt. Buildup of Germylidyne-bridged Tri- and Tetranuclear Clusters Reaction of organogermanium trihalides with KCo(CO)4 yields the trinuclear clusters RGeCo3(CO)9 (1, R Me, Ph, tBu) as well as the new tetranuclear clusters (RGe)2Co4(CO)11 (3, R Ph, tBu). The dinuclear complexes LnM GeI2 MLn (4–6, FeCp(CO)2, Co(CO)4, NiCpCO) resulting from insertion of GeI2 into metal-metal bonds react with KCo(CO)4 to form the clusters LnM GeCO3(CO)9 (7–9). Metal exchange reactions produce the hetero tetranuclear clusters (tBuGe)2Co3(CO)8M′Ln MoCp(CO)2, NiCp). Crystal structure analyses were performed for Cp(CO)2Fe GeCo3(CO)9 (7) and (tBuGe)2Co3(CO)8NiCp (11)." @default.
- W2036694945 created "2016-06-24" @default.
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- W2036694945 date "1985-05-01" @default.
- W2036694945 modified "2023-10-18" @default.
- W2036694945 title "Aufbau Germylidin‐verbrückter Drei‐ und Vierkerncluster" @default.
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- W2036694945 doi "https://doi.org/10.1002/cber.19851180503" @default.
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