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- W2036954631 abstract "Extended defects accomodating non-stoichiometry in rutiles reduced slightly to compositions of TiO1.9966, TiO1.9979, and TiO1.9986 are seen to dissolve in situ in an electron microscope using a goniometer at temperatures of up to 1000 °C. This allows to determine as directly as possible the stoichiometry dependence of the dissolution temperature, and hence the phase limits of nonstoichiometric TiO2−x. The defect structures formed during dissolution, and also the reprecipitation of extended defects upon cooling of the specimens to room temperature, are also studied. Dans un microscope électronique muni d'un porte-object chauffant jusqu' à des températures de 1000 °C environ, on a observé in situ la dissolution des défauts étendus accommodant la nonstoichiométrie de cristaux de rutile réduits aux compositions TiO1,9966, TiO1,9979 et TiO1,9986. Ceci a permis de déterminer la température de dissolution en fonction de l'écart à la stoichiométrie, et par là -měme la limite de la phase nonstoichiométrique TiO2−x aussi directement que possible. La structure des défauts formés durant la dissolution ainsi que la re-précipitation des défauts étendus (après dissolution) ont été également étudiées." @default.
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- W2036954631 date "1984-11-16" @default.
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- W2036954631 title "Extended versus small defect-equilibria in non-stoichiometric rutile. I. Dissolution and re-precipitation of extended defects observed by in-situ transmission electron microscopy" @default.
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- W2036954631 doi "https://doi.org/10.1002/pssa.2210860109" @default.
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