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- W2036955735 abstract "Summary A method for simultaneous quantitative determination of Mo(VI), Re(VII), Ru(III) and NO 3 - ions in aqueous solutions, using capillary zone electrophoresis (CZE) technique with direct UV detection, was developed. Electrophoretic mobility of Ru(III) ions in 0.1M NaHCO 3 solution was determined as 6.0×10 -8 m 2 V -1 s -1 at 25 °C. The best analytical characteristics of the developed method were achieved with a 100mM carbonate buffer solution containing 0.3mM TTAB, at a pH value of 9.8 and at an applied voltage of 10kV. Under these conditions, a linear relationship between the measured absorbance (λ=230nm) and the concentration of the species under study were observed in the range 5×10 -6 –10 -3 M for Mo(VI), 7×10 -6 –10 -3 M for Re(VII) and 10 -5 – -4 M for Ru(III). The minimum detectable concentrations were determined as 4.1×10 -6 M for NO 3 - , 5.2×10 -6 M for Mo(VI), 7.4×10 -6 M for Re(VII) and 1.0×10 -5 M for Ru(III). The accuracy of quantitative determination was estimated as 3%–5% for NO 3 - and 5%–6% for Mo(VI), Re(VII) and Ru(III) ions. The presence of 0.06M NaNO 3 (HNO 3 ) and of 10 -3 M U(VI) in the sample affected neither the detection limits of the species under study nor the selectivity of the method." @default.
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- W2036955735 date "2003-08-01" @default.
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- W2036955735 title "Determination of Mo(VI), Ru(III), Re(VII) and NO<sub>3</sub><sup>-</sup>in the solutions of nuclear fuel cycle by capillary electrophoresis" @default.
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- W2036955735 doi "https://doi.org/10.1524/ract.91.8.479.20003" @default.
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