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- W2037124639 abstract "The goal of this research was the synthesis and thermal characterization of poly(ester-siloxane) multiblock copolymers. Poly(butylene terephthalate) (PBT) was the polyester block. α, ω-Diamino-terminated poly(dimethylsiloxane) (PDMS) was reacted with an excess of dimerized fatty acid to form a dicarboxy-terminated oligomer containing stable amide links. Multiblock copolymers were obtained in a three-stage process: oligomer preparation, transesterification, and polycondensation from the melt. A magnesium-titanate catalyst was used for transesterification and polymer formation (polycondensation). The synthesized oligomer was considered to be the soft segment and its content ranged from 20 to 45% by weight. Multiblock copolymers showed microphase separation as determined by differential scanning calorimetry (DSC). Their morphology was studied by optical microscopy (OM) and showed spherulitic ordering." @default.
- W2037124639 created "2016-06-24" @default.
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- W2037124639 date "2000-01-01" @default.
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- W2037124639 title "Synthesis and thermal properties of poly(ester-siloxane) multiblock copolymers" @default.
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- W2037124639 doi "https://doi.org/10.1163/156855500300160276" @default.
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