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- W2037212076 abstract "In this paper we demonstrate experimentally that the continuously phase-modulated homonuclear decoupling sequence DUMBO-1 is suitable for high-resolution proton NMR spectroscopy of rigid solids. Over a wide range of experimental conditions, we show on the model sample L-alanine as well as on small peptides that proton linewidths of less than 0.5 ppm can be obtained under DUMBO-1 decoupling. In particular the DUMBO-1 sequence yields well resolved proton spectra both at slow and fast MAS. The DUMBO-1 decoupling scheme can in principle be inserted in any multi-nuclear or multi-dimensional solid-state NMR experiment which requires a high-resolution 1H dimension. An example is provided with the 13C-1H MAS-J-HMQC experiment." @default.
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- W2037212076 date "2003-07-01" @default.
- W2037212076 modified "2023-10-18" @default.
- W2037212076 title "Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling" @default.
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- W2037212076 doi "https://doi.org/10.1016/s1090-7807(03)00104-6" @default.
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