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- W2037223114 abstract "A novel NMR shift reagent, cobalt(III) meso-tetraphenylporphyrin (CoTPP) was used to determine the conformations of azacycloheptane and azacyclooctane ligands complexed to the metalloporphyrin. Using the observed ring current shifts and a previously calibrated ring current model, the best agreement between the observed and calculated ring current shifts for azacycloheptane was obtained for a chair conformation, in agreement with previous theoretical and experimental studies on the conformational stability of seven-membered rings. The ring current shifts for azacyclooctane are best interpreted in terms of a mixture of many conformations. These results suggest that CoTPP may be useful as a probe of other conformationally mobile ligands." @default.
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- W2037223114 title "NMR spectra of the porphyrins. 38—Conformational analysis of azacycloheptane and azacyclooctane using a novel cobalt(III) porphyrin shift reagent" @default.
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- W2037223114 doi "https://doi.org/10.1002/mrc.1260280412" @default.
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