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- W2037287862 abstract "Two methods are indicated for the determination of the metallic part of the total surface area of palladium-on-carrier catalysts from the chemisorption of carbon monoxide at room temperature. These methods are particularly suitable for use with a range of metal dispersions and/or concentrations in which measurements by other techniques, e.g., X-ray line broadening, small-angle scattering, and electron microscopy, cause difficulties. In cases where different techniques were suitable, good agreement was found with the results of carbon monoxide adsorption. Factors which may lead to erroneous results in the adsorption technique are the presence of residual oxygen or hydrogen on the palladium surface, and, in rare instances, sorption of carbon monoxide on the carrier. In the case of a 0.5% Pd-on-carrier catalyst the metal appeared to be so highly dispersed on the support that the ratio of adsorbed carbon monoxide molecules to palladium atoms was almost equal to unity." @default.
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- W2037287862 title "The determination of the free-metal surface area of palladium catalysts" @default.
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