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- W2037356064 abstract "Pd/Au hollow cone-like microstructures (HCMs) have been electrodeposited on indium tin oxide (ITO) using a two-step protocol, which involves the nucleation pulse and succedent constant potential reduction in the presence of metal precursors and polyvinylpyrrolidone (PVP). Scanning electron microscope (SEM), transmission electron microscope (TEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscope (XPS) were used to characterize the Pd/Au HCMs. The electrochemical results (cyclic voltammetry and chronoamperometry) testify that the Pd/Au HCMs exhibit significantly higher electrocatalytic activity and stability for the oxidation of formic acid than that of Pd/Au solid microhemispheres (SMHs). These attractive features are attributable to the unique hollow structures of Pd/Au with much higher electrochemical active surface areas and the exposure of favorable planes. Our work points to a new path for the preparation of Pd/Au HCMs, which are promising as electrocatalysts in direct formic acid fuel cell (DFAFC)." @default.
- W2037356064 created "2016-06-24" @default.
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- W2037356064 date "2011-07-01" @default.
- W2037356064 modified "2023-09-25" @default.
- W2037356064 title "Electrosynthesis of Pd/Au hollow cone-like microstructures for electrocatalytic formic acid oxidation" @default.
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- W2037356064 doi "https://doi.org/10.1016/j.electacta.2011.02.096" @default.
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