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- W2037367096 abstract "The novel quaternary reduced molybdenum oxides MTi0.7Mo0.3Mo5O10 (M = Sr, Eu) have been synthesized by solid-state reaction at 1400 °C for 48 h in sealed molybdenum crucibles. Their crystal structures were determined on single crystals by X-ray diffraction. Both compounds crystallize in the orthorhombic space group Pbca with 8 formula units per cell and the following lattice parameters: aSr = 9.1085 (7), bSr = 11.418 (1), and cSr = 15.092 (3) A; aEu = 9.1069 (7), bEu = 11.421 (2), and cEu = 15.075 (1) A. The Mo network is dominated by bioctahedral Mo10 clusters, which coexist randomly with Mo11 and Mo12 clusters (monocapped and bicapped Mo10 clusters). The Mo−Mo distances within the clusters range from 2.62 to 2.92 A and the Mo−O distances from 1.99 to 2.17 A as usually observed in the reduced molybdenum oxides. The Sr2+ and Eu2+ ions occupy large cavities, which result from the fusion of two cubooctahedra and thus are surrounded by 11 oxygen atoms. The M−O distances range from 2.50 to 3.23 A for the Sr c..." @default.
- W2037367096 created "2016-06-24" @default.
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- W2037367096 date "2010-05-25" @default.
- W2037367096 modified "2023-09-24" @default.
- W2037367096 title "ChemInform Abstract: MTi0.7Mo0.3Mo5O10 (M: Sr, Eu), First Evidence of Mono- and Bicapped Bioctahedral Mo11 and Mo12 Clusters: Synthesis, Crystal Structures, and Physical Properties." @default.
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- W2037367096 doi "https://doi.org/10.1002/chin.200132003" @default.
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