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- W2037585132 abstract "Abstract Complexes [(CO) 5 MC(OEt)(CCPh)] (M Cr ( 1a ), W ( 1b )) react with [PPh 4 ][HFe 3 (CO) 11 ] to give [PPh 4 ][Fe 3 (CO) 9 (μ 3 -η 3 - C(OEt)CCHPh] by a ligand transfer reaction. Complexes 1a and 1b react with octacarbonyldicobalt to give [((CO) 5 MC(OEt)CCPh)Co 2 (CO) 6 ] (M Cr( 3a ) or W ( 3b )), 3a being characterized by an X-ray structure determination. In boiling hexane, 3a and 3b rearrange to the clusters [MCo 2 (CO) 7 (μ-CO) 2 {μ 3 -η 4 -CC(OEt)CPhC(O)}](M Cr ( 4a ) or W ( 4b )) partially characterized by an X-ray structure determination for 4a and their isomers [MCo 2 (CO) 7 (μ- O) 2 {μ 3 -η 4 -CCPhC(OEt)C(O)}] (M Cr ( 5a ) or W ( 5b )) spectroscopically characterized." @default.
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- W2037585132 title "Study of the reactivity of the carbon-carbon triple bond in (CO)5MC(OEt)(CCPh) complexes (M Cr or W) towards [PPh4I[HFe3(CO)11] or [Co2(CO)8]: a ligand transfer reaction (Fe) or thermally induced build up of heterotrimetallic clusters (Co) bridged by the carbyne ligands C-C(OEt)CPhC(O)- or CCPhC(OEt)- C(O)-" @default.
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- W2037585132 doi "https://doi.org/10.1016/0022-328x(94)87277-5" @default.
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