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- W2037621911 abstract "The salt Diclofenac/ N -(2-hydroxyethyl) pyrrolidine when crystallizes from water forms a di-hydrate, which looses the crystallization water molecules on heating or in the presence of silica gel, undergoing a phase transition. The two processes were followed at room temperature, at 40 and 50°C by thermal analysis and analyzing the dimensional parameters obtained by scanning electron microscopy as a function of the changes occurring in the solid state. The fractal dimension of the particle surface ( D S ) was determined for the di-hydrate, the anhydrate and the anhydrous forms: D S values are close together suggesting that the processes modify only slightly the external morphology of the particles. The reactive dimension ( D R ) to dissolution suggests that the salt after the thermal treatment has a dissolution behaviour identical to that observed for the salt obtained from organic solvents. The two processes de-hydration and phase transition can be carried out at relatively low temperature, suggesting an important pathway to obtain the anhydrous form starting from the di-hydrate one." @default.
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- W2037621911 date "1999-04-01" @default.
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- W2037621911 title "Effect of the temperature on a hydrate diclofenac salt" @default.
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- W2037621911 doi "https://doi.org/10.1016/s0378-5173(99)00010-1" @default.
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