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• W2037653860 abstract "LiGayCo1-yO2 solid solutions, obtained under a high-pressure (3 GPa), were studied by high-frequency electron paramagnetic resonance (EPR) of Ni3+ spin probes and 71Ga MAS NMR. 71Ga MAS NMR experiments exhibit complex spectra that correspond to octahedral coordination and quadrupolar effects. For Ga-substituted oxides, high-frequency EPR of Ni3+ spin probes shows the existence of two new kinds of Ni3+ ions in tetragonally elongated octahedra with g⊥ > g∥. These ions are characterized by slightly different g-tensor and temperature of transition from dynamic to static Jahn−Teller effect. The extent of the local tetragonal distortion has been deduced from g∥. The reinforcement of the tetragonal distortion of NiO6 for LiGayCo1-yO2 as compared to LiCoO2 reflects the different structure characteristics of the GayCo1-yO2 and CoO2 layers. For Ga-rich composition, X-band EPR spectra exhibit a new signal with g ≈ 5 ascribable to high-spin Ni3+ located near defect sites. As compared to the Ga-free LiCoO2, a clipping effect in the slabs induced by the Ga inhibits the expansion of the c lattice parameter when LiGa0.1Co0.9O2 is oxidized." @default.
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• W2037653860 date "2003-04-09" @default.
• W2037653860 modified "2023-09-27" @default.
• W2037653860 title "Electron Paramagnetic Resonance and Solid-State NMR Study of Cation Distribution in LiGa<i>_y</i>Co₁_-<i>_y</i>O₂ and Effects on the Electrochemical Oxidation" @default.
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• W2037653860 doi "https://doi.org/10.1021/jp027807t" @default.
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