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- W2037654802 abstract "2,2,2-Trichloroethyl chloroformate and benzyl chloroformate cleave 1-benzyl-1,2,3,4-tetrahydro-2-methylisoquinolines of type 1 to yield tertiary stilbene urethanes of type 2 which are easily reduced or hydrogenolyzed to secondary amines. 6′-(Hydroxymethyl)-laudanosine (4) is converted by these reagents to the isochroman urethanes 11 and 12 which are split to yield the secondary amine 8 without the isochroman moiety being attacked. Spaltung von 1-Benzyl-tetrahydroisochinolinen über Urethane zu sekundären Aminen Chlorameisensäure-2,2,2-trichlorethylester bzw. Chlorameisensäurebenzylester spalten 1-Benzyl-1,2,3,4-tetrahydro-2-methylisochinoline vom Typ 1 zu tertiären Stilben-Urethanen vom Typ 2, die unter milden Bedingungen reduktiv bzw. hydrogenolytisch zu sekundären Aminen gespalten werden. 6′-Hydroxymethyllaudanosin (4) reagiert mit diesen Reagentien zu den Isochroman-Urethanen 11 bzw. 12, die ohne Angriff am Isochromanring zum sekundären Amin 8 umgesetzt werden." @default.
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- W2037654802 date "1984-01-01" @default.
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- W2037654802 title "Cleavage of 1-Benzyltetrahydroisoquinolines to Secondary Amines via Urethanes" @default.
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- W2037654802 doi "https://doi.org/10.1002/ardp.19843170512" @default.
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