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- W2037670601 abstract "Abstract 5,6-Anhydro-1,2- O -isopropylidene-α- D -glucofuranose ( 1 ) reacts smoothly with O , O -dialkylphosphoro-thioic and -dithioic acids and with diarylphosphinothioic acids, to give 6-substituted phosphinylthio and phosphinothioylthio derivatives in high yields. The reaction of 1 with the anions of O , O -dialkylphosphoro-thioic and -dithioic acids yields, quantitatively, the 5,6-episulphide with inversion of the configuration at C-5. A mechanism for this reaction is proposed, which involves a penta-covalent phosphorus intermediate." @default.
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- W2037670601 date "1980-08-01" @default.
- W2037670601 modified "2023-09-25" @default.
- W2037670601 title "O,O-dialkylphosphoro-thioic and -dithioic acids as functionalising reagents of monosaccharides: synthesis of 6-(dialkoxyphosphinylthio)-α-D-glucofuranoses, and a new route to 5,6-episulphides" @default.
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- W2037670601 doi "https://doi.org/10.1016/s0008-6215(00)85362-8" @default.
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