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- W2037850416 abstract "2D J—δ selective INEPT experiments were used to measure long-range 13C,1H coupling constants for the macrolide antibiotics roxithromycin, erythromycin and their metabolites, RU 39001 and erythralosamine, respectively. The 2D J—δ selective INEPT experiment was performed using selective excitation by a DANTE pulse train. In some cases, to avoid truncation problems in the t1 domain, treatment of the data using a linear prediction method was adopted. Dihedral angles for the glycosidic bonds and the erythronolid unit were deduced from a Karplus-type equation for conformational study. The apparent equilibrium between different conformers is discussed by comparison of experimental results and theoretical calculations by molecular dynamics." @default.
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- W2037850416 date "1994-01-01" @default.
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- W2037850416 title "Determination of long-range13C,1H coupling constants of macrolide antibiotics by 2DJ—δ selective INEPT experiments" @default.
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- W2037850416 doi "https://doi.org/10.1002/mrc.1260320102" @default.
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