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• W2037893706 startingPage "7756" @default.
• W2037893706 abstract "A series of three-dimensional (3D) octacyanometallate-based bimetallic magnets, {[Mn(H2O)][Mn0.75(HCOO)0.5(H2O)0.5][W(CN)8]·H2O}4n (1), {[Mn2(HCOO)(HCOOH)][M(CN)8]·H2O}n (M = W (2) and Mo (3)), and {[Mn2(HCOO)(HCOOH)][W(CN)8]·CH3OH}n (M = W (4) and Mo (5)), were synthesized by the reaction of octacyanometallates A3[M(CN)8]·nH2O (A = Na, Cs, and (C4H9)3NH; M = W and Mo; and n = 2 or 4) with manganese salt (Mn(CH3COO)2·4H2O, Mn(ClO4)2·6H2O, and MnCl2·4H2O) in aqueous or methanolic solution containing formic acid. All complexes crystallize in the tetragonal or orthorhombic system. Complex 1 shows an unexpected 3D network structure by connections of manganese ions and octacyanotangstate−manganese double layers via cyanide bridges, while other complexes have typical structure constructions similar to the reported complexes {[MnL]m[M(CN)8]}n (L = CH3COO−, Cl−, and H2O), which the CN group of [WV(CN)8] coordinates to eight MnII ions forming a −[W(CN)8]−Mn4−[W(CN)8]−Mn4− columnar chain, and then all chains share MnII ions as the nodes interlocking with each other to form the 3D networks. Magnetic studies indicate that the cyanide group mediates the antiferromagnetic coupling between octacyanometallates and manganese ions in all complexes, and the ferrimagnetic phase transition temperatures are 53, 52, 42, 49, and 41 K for 1−5, respectively." @default.
• W2037893706 created "2016-06-24" @default.
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• W2037893706 creator A5075995463 @default.
• W2037893706 date "2010-08-02" @default.
• W2037893706 modified "2023-10-17" @default.
• W2037893706 title "Manganese(II)-Octacyanometallate(V) Bimetallic Ferrimagnets with <i>T</i>_c from 41 to 53 K Obtained in Acidic Media" @default.
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• W2037893706 doi "https://doi.org/10.1021/ic100591h" @default.
• W2037893706 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/20677805" @default.
• W2037893706 hasPublicationYear "2010" @default.
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