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• W2037934831 abstract "Abstract A sample with a composition of 95 wt% Mg-5 wt% NbF 5 (named Mg-5NbF 5 ) was prepared by reactive mechanical grinding using Mg instead of MgH 2 as a starting material. Its hydriding and dehydriding rates were then measured under nearly constant hydrogen pressures. The activation of Mg-5NbF 5 was not required, and Mg-5NbF 5 had an effective hydrogen storage capacity, which was defined as the quantity of hydrogen absorbed for 60 min, of 5.50 wt%. At the first cycle ( n  = 1) at 593 K, the sample absorbed 4.37 wt% H for 5 min and 5.50 wt% H for 30 min under 12 bar H 2 , and desorbed 1.03 wt% H for 5 min, 4.66 wt% H for 30 min, and 5.43 wt% H for 60 min under 1.0 bar H 2 . Reactive mechanical grinding of Mg with NbF 5 , which formed MgH 2 , MgF 2 , NbH 2 , and NbF 3 by the reaction of 11 Mg + 7NbF 5  + 3H 2  → MgH 2  + 10MgF 2  + 2NbH 2  + 5NbF 3 , is considered to create defects, to produce reactive clean surfaces, and to reduce the particle size of Mg. The XRD pattern of Mg-5NbF 5 dehydrided at n  = 3 revealed Mg, small amounts of β-MgH 2 and MgO, and very small amounts of MgF 2 and NbH 2 . An increase in the dehydriding rate of Mg-5NbF 5 was attempted by adding Ni to Mg-5NbF 5 . Mg-5NbF 5 had higher initial hydriding and dehydriding (after the incubation period) rates and a larger effective hydrogen storage capacity than Mg-10NbF 5 , Mg-10MnO, and Mg-10Fe 2 O 3 , which were reported to have quite high hydriding rate and/or dehydriding rate." @default.
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• W2037934831 date "2014-10-01" @default.
• W2037934831 modified "2023-09-24" @default.
• W2037934831 title "Preparation and characterization of NbF 5 -added Mg hydrogen storage alloy" @default.
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• W2037934831 doi "https://doi.org/10.1016/j.ijhydene.2014.03.217" @default.
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