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• W2038165830 abstract "The high-pressure phases of solid ammonia have been investigated by x-ray diffraction in a diamond anvil cell at room temperature. Despite the first-order solid phase transition at $4phantom{rule{0.3em}{0ex}}mathrm{GPa}$, quasi-single crystals of ${mathrm{NH}}_{3}$ and ${mathrm{ND}}_{3}$ could be obtained and compressed to 123 and $62phantom{rule{0.3em}{0ex}}mathrm{GPa}$, respectively. The observed reflections above $4phantom{rule{0.3em}{0ex}}mathrm{GPa}$ are compatible with the structure determined by neutron diffraction on ${mathrm{ND}}_{3}$. We found strong evidence for an isosymmetric transition at $12phantom{rule{0.3em}{0ex}}mathrm{GPa}$ in ${mathrm{NH}}_{3}$ and $18phantom{rule{0.3em}{0ex}}mathrm{GPa}$ in ${mathrm{ND}}_{3}$. This transition is more likely due to rearrangements of the hydrogen atoms, whereas the N atoms remain on their quasi-hcp sites. The experimental equation of state (EOS) is compared to the one derived from first-principles calculations. A stiffening of the EOS above $55phantom{rule{0.3em}{0ex}}mathrm{GPa}$ could indicate the onset of a quantum-disordered regime for some of the H bonds." @default.
• W2038165830 created "2016-06-24" @default.
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• W2038165830 date "2006-05-11" @default.
• W2038165830 modified "2023-10-12" @default.
• W2038165830 title "Solid ammonia at high pressure: A single-crystal x-ray diffraction study to<mml:math xmlns:mml=http://www.w3.org/1998/Math/MathML display=inline><mml:mrow><mml:mn>123</mml:mn><mml:mspace width=0.3em /><mml:mi>GPa</mml:mi></mml:mrow></mml:math>" @default.
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• W2038165830 doi "https://doi.org/10.1103/physrevb.73.174111" @default.
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