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- W2038224521 abstract "A catalytic highly diastereo- and enantioselective synthesis of 2,6-cis-substituted tetrahydropyrans was realized using a one-pot sequential catalysis involving Henry and oxa-Michael reactions. The nitroaldol products obtained in a highly enantioselective copper(II)-catalyzed Henry reaction between nitromethane and 7-oxo-hept-5-enals were subsequently treated with a catalytic amount of camphorsulfonic acid (CSA) to give the desired tetrahydropyran derivatives in excellent yields, diastereoselectivities (dr >99:1), and enantioselectivities (ee = 98–99%). The reaction can also be used for the high stereoselective synthesis of a cis-2,6-disubstituted morpholine." @default.
- W2038224521 created "2016-06-24" @default.
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- W2038224521 date "2013-06-11" @default.
- W2038224521 modified "2023-09-25" @default.
- W2038224521 title "Highly Stereoselective Synthesis of 2,6-<i>cis</i>-Substituted Tetrahydropyrans Using a One-Pot Sequential Catalysis" @default.
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- W2038224521 doi "https://doi.org/10.1021/ol400900h" @default.
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