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- W2038324076 abstract "Abstract The proton NMR second moment and spin-lattice relaxation time for polycrystalline tetraethyl-and tetrabutylammonium perchlorates have been measured over a wide range of temperatures. Solid-solid phase transitions related to the onset of cation tumbling were found for both compounds and confirmed by DSC. In the low temperature phases methyl-group reorientation was evidenced. For tetrabutylammonium cation a dynamic nonequivalence of one methyl group is found. The geared motion of the alkyl chains related with the onset of successive CH 2 -group reorientations is suggested." @default.
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- W2038324076 date "1994-03-01" @default.
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- W2038324076 title "Molecular Motion in Solid Tetraethyl-and Tetrabutylammonium Perchlorates" @default.
- W2038324076 doi "https://doi.org/10.1515/zna-1994-0303" @default.
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