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• W2038476908 abstract "A series of investigations of electrolytic coloration effects produced in MgO single crystals containing iron-group impurities has been carried out. The purpose of these investigations was to determine the identity and production mechanism of localized coloration or dark streaks that are frequently observed following the electrical breakdown of MgO crystals at temperatures in the range of 1000°C. A technique employing a point contact cathode was used to reproduce these coloration effects in a controlled systematic manner. Studies using a variety of techniques (MCD, EPR, SIMS, light scattering, etc.) establish that the formation of metallic precipitates by electrolytic reduction of impurities is primarily responsible for the observed localized dark coloration effects. In situ observations of the coloration process showed that it was initiated at the cathode and that the regions of coloration are coincident with those regions of the MgO crystal where the catastrophic failure in electrical insulating properties occurs. Electrical breakdown and coloration effects were observed in MgO crystals doped with each member of the entire 3d transition series except scandium. Crystals doped with different impurities did vary, however, in their tendency to fail electrically. Similar solid state chemical alterations were induced by more conventional reduction techniques which generally required higher temperatures to produce metallic colloids than electrolysis." @default.
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• W2038476908 date "1984-01-01" @default.
• W2038476908 modified "2023-09-27" @default.
• W2038476908 title "Electrolytic coloration and electrical breakdown of MgO single crystals" @default.
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• W2038476908 doi "https://doi.org/10.1016/0022-4596(84)90310-4" @default.
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