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- W2038501935 abstract "The nitromethane addition to 1,2-O-isopropylidene-5-O-trityl-α-D-erythro-pentofuranos-3-ulose (1) proceeded smoothly to give the corresponding branched-chain sugar (2), which on acetylation afforded (3) followed by elimination of acetic acid in presence of a base catalyst, resulted in the formation of the corresponding nitro olefin (4). The nitro olefin when subjected to borohydride reduction gave 5-O-acetyl-3-deoxy-1,2-O-isopropylidene-3-(nitromethyl)-α-D-ribofuranose (5), which on catalytic hydrogenation followed by acetylation yielded the 3-(acetamidomethyl)-5-O-acetyl-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose (6). By the study of the NMR spectra of 3-deoxy derivatives (5) and (6), their D-ribo configurations were established." @default.
- W2038501935 created "2016-06-24" @default.
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- W2038501935 date "1977-06-01" @default.
- W2038501935 modified "2023-09-25" @default.
- W2038501935 title "Branched-Chain Deoxy Nitro and Amino Sugar Derivatives from Ketose" @default.
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- W2038501935 doi "https://doi.org/10.1246/bcsj.50.1619" @default.
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