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- W2038530379 abstract "Abstract High-performance liquid chromatographic detection of UV-chromophore-deficient organophosphorus compounds has been aided by a new post-column photolysis-molybdate procedure. In the new procedure, a methanolic, acidified molybdate reagent is added to the eluent just prior to a photolysis chamber consisting of crocheted Teflon tubing wrapped around a mercury-discharge lamp. Organophosphorus compounds are photolyzed to orthophosphate, which in turn reacts with molybdate to form 12-molybdophosphoric acid (12-MPA). The 12-MPA is reduced photolytically to a molybdenum-blue species that absorbs at 735 nm. Because a photoinitiator (such as peroxydisulfate) is not needed, only one reagent pump is required. A limit of detection of about 10 ppb was indicated for a diphosphonate." @default.
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- W2038530379 date "1995-11-01" @default.
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- W2038530379 title "Preliminary Examination of A New Post-Column Photolysis-Molybdate Reaction Detection System for the Determination of Organophosphorus Compounds By High Performance Liquid Chromatography" @default.
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- W2038530379 doi "https://doi.org/10.1080/10739149508014120" @default.
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