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- W2038748811 abstract "A new short strategy to prepare the spiroketal fragment of calyculins is presented. A novel Seyferth–Gilbert type homologation of hindered lactols to the corresponding alkynes has been achieved for the first time. The spirocyclization was achieved efficiently via a DIHMA (double intramolecular hetero-Michael addition) process of this hindered ynone. The spirocyclization rate is not dependent on the stereochemistry of the alkoxy substituent in the oxolane ring." @default.
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- W2038748811 date "2004-10-01" @default.
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- W2038748811 title "An expedient synthesis of spiroketals: model studies for the calyculin C16–C25 fragment" @default.
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- W2038748811 doi "https://doi.org/10.1016/j.tet.2004.07.059" @default.
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