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- W2038785612 abstract "Solvothermal reactions of Zn(NO3)2, 1,4-benzenedicarboxylic acid (H2bdc), and 4,4′-azopyridine (azpy) in different conditions yielded [Zn(bdc)(bphy)]·DMF·H2O (1a, bphy = 1,2-bis(4-pyridyl)hydrazine, DMF = N,N-dimethylformamide) and [Zn(bdc)(bphy)]·EtOH·H2O (1b) with two-fold interpenetrated dmp topology and [Zn2(bdc)2(bphy)]·1.5EtOH·H2O (2a) and [Zn2(bdc)2(bphy)]·DMA·1.5H2O (2b, DMA = N,N-dimethylacetamide) with two-fold interpenetrated pcu topology. The in situreduction of azpy to bphy was confirmed by single-crystal structures and LC-MS analyses of the acid-digested crystalline samples, as well as controlled solvothermal experiments. Removal of the guest molecules in 1a/1b and 2a/2b converts the materials to guest-free phases [Zn(bdc)(bphy)] (1) and [Zn2(bdc)2(bphy)] (2), respectively, which were identified by PXRD. CO2 sorption experiments performed at 195 and 298 K showed low porosity for 1 and gated sorption behavior for 2. At 298 K, 2 exhibits high selectivity for adsorbing CO2 over CH4." @default.
- W2038785612 created "2016-06-24" @default.
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- W2038785612 date "2011-01-01" @default.
- W2038785612 modified "2023-09-25" @default.
- W2038785612 title "Flexible porous coordination polymers constructed from 1,2-bis(4-pyridyl)hydrazine via solvothermal in situ reduction of 4,4′-azopyridine" @default.
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- W2038785612 doi "https://doi.org/10.1039/c1dt10682a" @default.
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