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• W2038856788 abstract "Abstract (1,10-phenanthroline)bis(1,2,3,4-tetrahydroquinolinecarbodithioato-S,S′)mercury(II); [Hg(thqdtc) 2 (1,10-phen)] (1); has been synthesized and characterized by elemental analysis, IR and NMR spectroscopy and single crystal X-ray analysis. IR spectrum of the complex reveals the contribution of thioureide form to the structure. In the 13 C NMR spectrum, [Hg(thqdtc) 2 (1,10-phen)] shows a single low-field resonance associated with backbone carbon of dithiocarbamate (N 13 CS 2 ) at 205.7 ppm. The mononuclear structure of [Hg(thqdtc) 2 (1,10-phen)] exhibits monodentate and bidentate coordination by dithiocarbamate ligands and an intermediate geometry between tetragonal pyramidal and trigonal bipyramidal for mercury, defined by an N 2 S 3 donor set. [Hg(thqdtc) 2 (1,10-phen)] has been found to be an effective single-source precursor for the preparation of α-HgS nanosheets via solvothermal method. The as-prepared HgS nanosheets have been characterized by powder XRD, TEM, UV–Vis and fluorescence spectroscopy. TEM image of HgS exhibits that the as-prepared HgS particles are hexagonal shaped nanosheets. UV–Vis spectroscopy established pronounced quantum confinement effect." @default.
• W2038856788 created "2016-06-24" @default.
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• W2038856788 date "2014-11-01" @default.
• W2038856788 modified "2023-09-24" @default.
• W2038856788 title "Synthesis of α-mercury sulfide nanosheets from (1,10-phenanthroline)bis(1,2,3,4-tetrahydroquinolinecarbodithioato-S,S′)mercury(II)" @default.
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• W2038856788 doi "https://doi.org/10.1016/j.molstruc.2014.07.083" @default.
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