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- W2039060147 abstract "Abstract A series of tetranuclear Mo4S4(R2NCS2)6 complexes has been prepared by using the ‘self-assembly’ route as well as by synthesis from well-defined molecular building blocks. A variety of mononuclear, dinuclear and trinuclear building blocks have been successfully used to prepare the tetranuclear Mo4S46+ complexes. These thiocubanes have been prepared with mono-anionic 1,1-dithiolate ligands, which provide each of the Mo atoms with a pseudo-octahedral coordination geometry and result in the formation of neutral species. Mo4S4L6 complexes with dialkyldithiocarbamate (DTC), R2NCS2; dialkyldithiophosphate (DDP), (RO)2PS2; alkylxanthate (XAN), ROCS2; and alkylthioxanthate (THIOXAN), RSCS2 ligands have been prepared. The structure of the Mo4S4(DDP)6 complex was determined by single crystal X-ray structure analysis and is compared with the structures of other known Mo4S4 thiocubane complexes. The synthesis, electrochemistry, reactivity and bonding of the tetranuclear clusters are presented." @default.
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- W2039060147 date "1992-08-01" @default.
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- W2039060147 title "Synthesis and reactivity of molybdenum-sulfur cubes" @default.
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- W2039060147 doi "https://doi.org/10.1016/s0020-1693(00)92400-9" @default.
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