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- W2039690129 abstract "Morphological and differential thermal analysis (d.t.a.) studies show that the melting temperature of the principal crystalline lamellar phase (phase I) of PEO-Nal and PEO-NaSCN complexes (which is ∼463K for a high polymer) is independent of the nature of the anion. However, n.m.r. and conductivity measurements indicate that mesophase behaviour occurs in phase I above ∼333K in NaSCN-PEO and ∼363K in Nal-PEO. This temperature region marks the onset of an ionic conduction process of lower activation energy. The disordering of a second complexed phase (phase II) which forms in the interlamellar regions of the linear complexes and within the network of a crosslinked PEO gel is considered to account for the 325–340K endotherms which are observed in these materials. In particular, annealed and melt recrystallized NaSCN complexes with high molecular weight PEO form banded morphological features consisting of stacks of lamellar fragments which are indicative of rigid and stable molecular units. The ionic conductivities of saturated (excess salt) and stoichiometric linear complexes are compared with that of the complexed network which has the greater ambient temperature conductivity." @default.
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- W2039690129 date "1982-05-01" @default.
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- W2039690129 title "Morphology and ionic conductivity of complexes of sodium iodide and sodium thiocyanate with poly(ethylene oxide)" @default.
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