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- W2039730902 abstract "The alkali tricyanomelaminate monohydrates M3[C6N9]·H2O with M=K, Rb were synthesized by aqueous ion exchange starting from anhydrous Na3[C6N9] and KCl or RbCl, respectively. The crystal structure of Rb3[C6N9]·H2O was solved on the basis of synchrotron X-ray powder diffraction data and refined by the Rietveld method (P1, Z=1, a=393.17(1), b=826.48(2), c=1036.28(3) pm, α=70.798(1), β=81.872(2), γ=87.504(1)°, wRp=0.016, Rp=0.011, RF=0.043). K3[C6N9]·H2O was found to be isotypic and its crystal structure was refined by the Rietveld method on the basis of conventional X-ray powder diffraction data (a=372.91(2), b=809.20(5), c=1012.22(5) pm, α=71.209(2), β=80.524(3), γ=86.653(3)°, wRp=0.084, Rp=0.064, RF=0.052). Both compounds contain M+ ions, cyclic tricyanomelaminate ions [C6N9]3− and H2O molecules. The salts were characterized by vibrational spectroscopy (FTIR and Raman). According to thermogravimetric investigations the monohydrates lose their crystal water between 80–180 °C (K3[C6N9]·H2O) and 60–200 °C (Rb3[C6N9]·H2O), respectively, yielding the respective anhydrous tricyanomelaminates M3[C6N9] (M=K, Rb)." @default.
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- W2039730902 date "2002-10-01" @default.
- W2039730902 modified "2023-09-26" @default.
- W2039730902 title "Synthesis, crystal structure determination from X-ray powder diffractometry and vibrational spectroscopy of the tricyanomelaminate monohydrates M3[C6N9]·H2O (M=K, Rb)" @default.
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- W2039730902 doi "https://doi.org/10.1016/s1293-2558(02)00012-2" @default.
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