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- W2039793443 abstract "Reaction of tin(II) chloride with RNa(THF)2 (R = tBu3Si) in THF at –30 °C led to a complex reaction mixture, from which the compounds R4Sn4(THF)2, R2SnSnR2 (5), R–R (7), and a brownish black compound 6 were isolated. In toluene as solvent, the zwitterionic distannene 5 was obtained together with 7 and 6 which upon treatment with Et3PX, furnished the cluster compounds (RSnX)4 (10: × = Se; 11: × = Te). The X-ray structure analyses of the isotypic compounds 10 and 11 revealed that the tin atoms occupy the corners of an undistorted tetrahedron with weak tin–tin interactions. The chalcogen atoms form a plane which bisects the Sn4 tetrahedron." @default.
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- W2039793443 date "1998-09-01" @default.
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- W2039793443 title "A Zwitterionic Distannene and Two (RSnX)4 Cages with an Unusual Arrangement of the Sn4X4 Cluster Atoms (R =tBu3Si, × = Se, Te)" @default.
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- W2039793443 doi "https://doi.org/10.1002/(sici)1099-0682(199809)1998:9<1333::aid-ejic1333>3.0.co;2-f" @default.
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