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- W2039863073 abstract "Abstract The crystallographic structure of the binary uranium germanide U 3 Ge 5 was determined from single crystal X-ray diffraction data to R ( F )=0.076 and R ω =0.085. U 3 Ge 5 crystallizes with the hexagonal AlB 2 structure type ( P6/mmm ) with the following lattice parameters: a =3.954(1) A, c =4.125(1) A. A partial occupation of the germanium site leads to the effective composition UGe 1.57 and the observation of weak superlattice reflections indicates some ordering of the germanium vacancies which could not be resolved. Magnetic susceptibility measurements on an annealed polycrystalline sample revealed ferromagnetic ordering below T c =94 K, which was previously claimed for the composition U 3 Ge 4 . The magnetic structure was determined from neutron powder diffraction data collected on the G4-1 powder diffractometer at LLB Saclay. The structure is ferromagnetic ( R m =0.02) with the uranium moments at 1.4 K: M U =2.28(4) μ B , described by a main component along the c -axis of the hexagonal subcell M z =1.80(4) μ B and an in-plane component: M x,y =1.40(5) μ B ." @default.
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- W2039863073 date "1999-02-01" @default.
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- W2039863073 title "Crystal and magnetic structure of the binary uranium germanide U3Ge5" @default.
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- W2039863073 doi "https://doi.org/10.1016/s0925-8388(98)00873-1" @default.
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