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- W2040100874 abstract "Tellurium(IV) oxide (TeO2) reacts with nonconjugated dienes in acetic acid at reflux temperature in the presence of lithium halide or iodine to give the corresponding vic-diacetates in moderate yields. When the reaction is carried out at 80°C and the reaction mixture is then reduced with aqueous sodium thiosulfate, bis(β-acetoxyalkyl)ditellurides are isolated as main products. Treatment of the ditellurides with refluxing acetic acid affords the corresponding vic-diacetates in good yields. The expected tellurium containing heterocyclic compounds, such as telluracyclopentanes and telluracyclohexanes, are not formed and/or isolated under the conditions employed. When 4-vinylcyclohexene and limonene are used as dienes in the diacetoxylation reaction, aromatic compounds due to the dehydrogenation of cyclohexene ring are also produced in moderate yields." @default.
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- W2040100874 date "1995-02-01" @default.
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- W2040100874 title "Diacetoxylation of nonconjugated dienes with TeO2 and the isolation of intermediate organotellurium compounds" @default.
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- W2040100874 doi "https://doi.org/10.1016/0022-328x(94)05001-r" @default.
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