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• W2040230061 abstract "A suitable combination of synthetic design, orthogonal protecting groups and coupling reagents was used to complete the first known synthesis of the natural marine cyclodepsipeptide IB-01212. The cyclic, symmetric octapeptide contains two of each of the following residues: L-N,N-Me2Leu, L-Ser, L-N-MeLeu and L-N-MePhe. IB-01212 also features two symmetric ester bonds between the hydroxyl group of Ser and the carboxyl function of the N-MePhe. Total solid-phase syntheses of the product was performed in parallel via three distinct routes: dimerization of heterodetic fragments, linear synthesis, and convergent synthesis. The convergent strategy gave the best results in terms of product yield and purity and is particularly suitable for the large-scale synthesis of IB-01212 and similar peptides." @default.
• W2040230061 created "2016-06-24" @default.
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• W2040230061 date "2005-11-30" @default.
• W2040230061 modified "2023-10-14" @default.
• W2040230061 title "Total Solid-Phase Synthesis of Marine Cyclodepsipeptide IB-01212" @default.
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• W2040230061 doi "https://doi.org/10.1021/jo051601h" @default.
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