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• W2040247755 abstract "The protonolysis of group 4 M(IV)(OR)4, M = Ti, Zr, organic alkyl- or aryloxides with the cluster acid (CO)9Co3(μ3-CCO2H) leads to a series of novel tricobalt cluster M(IV) alkoxy- or aryloxycarboxylates, most of which contain bridging oxo ligands. The compounds, which are isolated in good yield as crystalline substances and characterized spectroscopically as well as crystallographically, are Zr2(μ-OCH(CH3)2)2(OCH(CH3)2)2{μ-(CO)9Co3(μ3-CCO2)}2{(CO)9Co3(μ3-CCO2)}2, 1; Ti4(μ3-O)4(OR)4{μ-(CO)9Co3(μ3-CCO2)}4, 2 (R = CH(CH3)2, 2a; (CH2)3CH3, 2b; C6H5,2c; 2,6-(CH3)2-C6H3, 2d); Ti6(μ3-O)4(μ-OCH2CH3)4(OCH2CH3)8{μ-(CO)9Co3(μ3-CCO2)}4, 3; and [Ti6(μ3-O)2(μ-O)2(μ-OCH(CH3)2)2(OCH(CH3)2)2(1,2-O2C6H4)4{μ-(CO)9Co3(μ3-CCO2)}4], 4. Further, the mixed-metal derivatives [Ti2Co2{(OCH2)3CCH3}2(OCH(CH3)2)2{μ-(CO)9Co3(μ3-CCO2)}4], 5, and [{Co3Ti(OCH3)6(HOCH3)(THF){μ-(CO)9Co3(μ3-CCO2)}3}2(O2CCO2)]·2HOCH3·2THF,6, in which the Co(II) ions are derived from in situ tricobalt cluster degradation, are characterized in similar fashion...." @default.
• W2040247755 created "2016-06-24" @default.
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• W2040247755 date "1997-11-01" @default.
• W2040247755 modified "2023-10-16" @default.
• W2040247755 title "Clusters as Ligands. 5. Tricobalt Cluster Alkoxycarboxylates of Titanium and Zirconium Exhibiting Novel Structures and Properties" @default.
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• W2040247755 doi "https://doi.org/10.1021/om970837b" @default.
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