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- W2040275715 abstract "The polymerization of 1,3-dioxolane in solution in methylene chloride, catalysed by antimony pentafluoride, fluorosulphonic and perchloric acids, azonenzene perchlorate or a mixture of antimony pentafluoride and fluorosulphonic acid, has been found to be an autocatalytic process. A kinetic analysis of the autocatalytic polymerization of 1,3-dioxolane under the influence of boron trifluoride etherate has been made. The ratio of the rate constants of reaction of the catalyst with a polymer chain unit and with a monomer molecule was determined. The rate constant for the formation of active centres by reaction of Et 2 O·BF 3 with the polymer has been determined by the method of degradation of the polydioxolane. The mechanism of reaction of Lewis acids with the monomer and with the polymer molecule is discussed." @default.
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- W2040275715 date "1975-01-01" @default.
- W2040275715 modified "2023-09-25" @default.
- W2040275715 title "The participation of macromolecules in generation of active centres in polymerization of cyclic acetals" @default.
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- W2040275715 doi "https://doi.org/10.1016/0032-3950(75)90245-2" @default.
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