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- W2040280535 abstract "Amylose-grafted chitin and chitosan were synthesized by chemoenzymatic methods according to the following reaction manners. First, maltoheptaose was introduced to chitosan by a reductive amination using sodium cyanotrihydroborate in a mixed solvent of 1.0 mol/L aqueous acetic acid and methanol at room temperature to produce a maltoheptaose-grafted chitosan (1). The functionality of maltoheptaose to chitosan in 1 depended on reaction time. The phosphorylase-catalyzed enzymatic polymerization of α-d-glucose 1-phosphate was then performed from 1 to obtain amylose-grafted chitosan (2). Maltoheptaose-grafted chitin (3) was synthesized by N-acetylation of 1 using acetic anhydride in a mixed solvent of aqueous acetic acid and methanol. Then, synthesis of amylose-grafted chitin (4) was performed by the phosphorylase-catalyzed enzymatic polymerization under conditions the same as those for 2. The average DPs of amylose graft chains in 2 and 4 depended on the feed ratios of α-d-glucose 1-phosphate to maltoheptaose primers in 1 and 3." @default.
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- W2040280535 date "2007-11-16" @default.
- W2040280535 modified "2023-10-14" @default.
- W2040280535 title "Chemoenzymatic Syntheses of Amylose-Grafted Chitin and Chitosan" @default.
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- W2040280535 doi "https://doi.org/10.1021/bm701000t" @default.
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