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• W2040281982 abstract "A combination of variable temperature X-ray powder diffraction, ac impedance spectroscopy and differential thermal analysis (DTA) has been used to characterise phase transitions in the Bi2ZrxV1−xO5.5−(x/2)−δ, BIMEVOX system. At low substitution levels α-, β-, and γ-phase BIMEVOX structures are observed as a function of temperature with some evidence for an intermediate phase, ɛ, seen between β and γ phases on heating. At x = 0.10 the β-phase is observed at room temperature with a transition to the γ-phase at around 500 °C. There is evidence for a subtle phase transition at around 200 to 250 °C in the variation of refined cell parameters and the Arrhenius plot of conductivity for this composition that may be associated with a vacancy ordering phenomenon. For the x = 0.19 composition, despite near equivalence of a and b unit cell parameters, variation in the unit cell c-parameter, DTA and Arrhenius plots of conductivity show evidence of a β↔γ transition between 450 and 500 °C and that the true symmetry of the low temperature phase is likely to be orthorhombic." @default.
• W2040281982 created "2016-06-24" @default.
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• W2040281982 date "2005-06-01" @default.
• W2040281982 modified "2023-10-09" @default.
• W2040281982 title "Phase transitions in the BIZRVOX system" @default.
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• W2040281982 doi "https://doi.org/10.1016/j.ssi.2005.04.024" @default.
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