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- W2040295426 abstract "[Fe(C5Me5)2][Au(C3S5)2] (1) (C3S52−=4,5-dimercapto-1,3-dithiol-2-thionate) has been prepared by a reaction of [NBun4][Au(C3S5)2] with [Fe(C5Me5)2][BF4] in N,N-dimethylformamide. [NBun4][Au(C3S5)2] has been oxidized electrochemically in the presence of Fe(C5Me5)2 and Fe(C5H5)2 in acetonitrile to afford [Fe(C5Me5)2]0.33[Au(C3S5)2] (2) and [Fe(C5H5)2]0.33[Au(C3S5)2] (3). A single-crystal X-ray structure analysis of 1 reveals that dimeric units of the [Au(C3S5)2]− anion have one-dimensional arrangement through sulfur-sulfur contacts in the crystal phase. The triclinic crystal, space group P1, has cell dimensions a = 11.675(5), b = 15.118(6), c = 10.066(4) Å, α = 85.50(4), β = 94.63(4), γ = 68.87(3)° and Z = 2. The refinement based on 5804 reflections (|Fo|>3σ(F)) converged at R = 0.042. The partially oxidized species 2 and 3 exhibit electrical conductivities of 0.093 and 0.12 S cm−1, respectively, measured for compacted pellets at 25°C and their molecular interactions described based on electronic reflectance and X-ray photoelectron spectra." @default.
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- W2040295426 date "1992-03-01" @default.
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- W2040295426 title "X-ray crystal structure of [Fe(C5Me5)2][Au(C3S5)2] and properties of partially oxidized [Au(C3S5)2] anion complexes" @default.
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- W2040295426 doi "https://doi.org/10.1016/s0020-1693(00)80344-8" @default.
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