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- W2040320662 abstract "An efficient method has been developed to prepare all four isomers of the hydroxyl derivatives of sibutramine by addition of Grignard reagents (R)- or (S)-5 to a single enantiomer of sulfinyl imine (R)-1 simply by tuning the reaction solvent. The phenomenon of the reversed diastereoselectivity in CH2Cl2 and THF implied that the reaction may proceed through a chelated cyclic transition state in CH2Cl2 and nonchelated acyclic transition state in THF." @default.
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- W2040320662 date "2005-05-25" @default.
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- W2040320662 title "Control of Diastereoselectivity by Solvent Effects in the Addition of Grignard Reagents to Enantiopure <i>t</i>-Butylsulfinimine: Syntheses of the Stereoisomers of the Hydroxyl Derivatives of Sibutramine" @default.
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- W2040320662 doi "https://doi.org/10.1021/ol0507017" @default.
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