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- W2040434842 abstract "Abstract The thermal dehydration of NiSeO4·6H2O, NiSeO4·4H2O and NiSeO4·H2O has been studied by TG, DTA and DSC. The dehydration of NiSeO4·6H2O depends on both the heating rate and the sample mass. The following intermediate hydrates are produced: NiSeO4·5H2O; NiSeO4·4H2O; NiSeO4·2H2O; NiSeO4·H2O and NiSeO4·0.5H2O. The enthalpies of dehydration of these stages have been determined. The enthalpies of formation of NiSeO4·6H2O; NiSeO4·4H2O and NiSeO4·H2O (amorphous and crystalline) as well as the enthalpy of transformation of amorphous NiSeO4·H2O into crystalline NiSeO4·H2O have been calculated from DSC data. The lattice parameters of NiSeO4·4H2O and NiSeO4·2H2O have been calculated. NiSeO4·4H2O crystallizes in the monoclinic system with lattice parameters: a = 5.959(3) A ; b = 13.771(8) A ; c = 8.023(5) A ; β = 90.66(6)∘; V = 658.3(5) A 3 ; SG P21/n. NiSeO4·2H2O forms orthorhombic crystals with lattice parameters: a = 10.351(4) A ; b = 10.219(4) A ; c = 9.017(5) A ; V = 953.9(6) A 3 ." @default.
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- W2040434842 date "1997-01-01" @default.
- W2040434842 modified "2023-09-27" @default.
- W2040434842 title "TG, DTA, DSC and X-ray powder diffraction studies on some nickel selenate hydrates" @default.
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- W2040434842 doi "https://doi.org/10.1016/s0040-6031(96)03062-6" @default.
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