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• W2040473346 abstract "Chemical shift anisotropy (CSA) is an immensely useful interaction to study the structure, dynamics, and function of a wide variety of chemical and biological molecules. Traditionally the only unambiguous way to determine both the principal values and the orientation of the principal axes of the CSA tensor has been to follow the chemical shift frequency changes as a crystal of known structure is rotated relative to the direction of the external magnetic field. This classic method employs rotations about three mutually orthogonal axes of a single crystal. It is shown here that just two, or one, of the above rotations suffice to determine the CSA tensor orientation by borrowing, the easy to obtain, principal values of CSA from an independent source. Methods for using two rotation patterns or even a single rotation pattern are described and illustrated with known chemical shielding tensors." @default.
• W2040473346 created "2016-06-24" @default.
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• W2040473346 date "2002-04-01" @default.
• W2040473346 modified "2023-09-26" @default.
• W2040473346 title "Determination of the Chemical Shielding Tensor Orientation from Two or One of the Three Conventional Rotations of a Single Crystal" @default.
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• W2040473346 doi "https://doi.org/10.1006/jmre.2002.2518" @default.
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