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- W2040480724 abstract "A five-step conversion of IrCl(CO)(PPh3)2 into IrCl(CSe)(PPh3)2 via Ir(η2-CSe2)Cl(CO)(PPh3)2 is described. IrCl(CSe)(PPh3)2 is oxidized by Cl2 to IrCl3(CSe)(PPh3)2 and by O2 to Ir(η2-O2)Cl(CSe)(PPh3)2, and reaction with Ag+ in MeCN gives [Ir(CSe)(MeCN)(PPh3)2]+. NaBH4 in the presence of PPh3 reduces IrCl(CSe)(PPh3)2 completely to IrH2(SeMe)(PPh3)3 and the η2-CSe2 adduct, Ir(η2-CSe2)Cl(CSe)(PPh3)2, with MeI forms the metallacycle [Ir(C[SeMe]SeC[SeMe])I2(PPh3)2]+." @default.
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- W2040480724 date "1983-08-01" @default.
- W2040480724 modified "2023-09-27" @default.
- W2040480724 title "Selenocarbonyl complexes of iridium(I) and iridium(III). Synthesis and reactions of IrCl(CSe)(PPh3)2" @default.
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- W2040480724 doi "https://doi.org/10.1016/s0022-328x(00)99848-6" @default.
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