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- W2040558686 abstract "Nanocomposites were synthesized from polyamide and aminosilane functionalized montmorillonite through solution intercalation method. Polyamide resin was prepared by reacting a mixture of p-phenylenediamine and 4,4′-oxydianiline with isophthaloyl chloride (IPC) in N,N′-dimethyl acetamide (DMAc) under anhydrous conditions. The resulting chains were end capped with carbonyl chloride using slight excess of IPC near the end of reaction. 3-Aminopropyltriethoxysilane (APTS) was used for the surface modification of clay. Triethoxysilane groups of APTS promoted the reaction between silane and hydroxyl groups on the surface of clay. The compatibility between the two disparate phases was achieved through interaction of free amine groups of modified clay with carbonyl chloride of the matrix. Thin films obtained by evaporating the solvent were characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM), Transmission electron microscopy (..." @default.
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- W2040558686 date "2014-12-13" @default.
- W2040558686 modified "2023-09-24" @default.
- W2040558686 title "Preparation and Properties of Nanocomposites Derived from Aromatic Polyamide and Surface Functionalized Nanoclay" @default.
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- W2040558686 doi "https://doi.org/10.1080/00986445.2014.990634" @default.
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