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- W2040573218 abstract "Two new stable isotope dilution assays were developed for the quantification of ochratoxin A in human blood samples for exposure studies. The methods based on two different sample extraction and cleanup procedures including liquid–liquid extraction with following immunoaffinity chromatography (IA) as well as a dispersive solid-phase extraction (DSPE) method. For detection, LC–MS/MS was applied. For the first time, exact quantitation of the reference compound ochratoxin A was performed by quantitative NMR spectroscopy (qNMR). Additionally, a comparison of different blood-drawing procedures revealed no differences for heparin plasma and serum whereas citrate plasma gave significantly lower results for the mycotoxin. Limits of detection (LOD: 0.02 ng/g (IA) vs 0.03 ng/g (DSPE)), limits of quantification (LOQ: 0.07 ng/g (IA) vs 0.08 ng/g (DSPE)), relative recovery (⩾94%), precision, and linearity indicated excellent performance of the developed methods." @default.
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- W2040573218 date "2011-12-01" @default.
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- W2040573218 title "Development of stable isotope dilution assays for ochratoxin A in blood samples" @default.
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- W2040573218 doi "https://doi.org/10.1016/j.ab.2011.08.032" @default.
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